One-way reaction/distillation units
Batch reactor for stirring under normal pressure or vacuum, with possibility of addition of liquids and boiling under reflux. The descending condenser with intermediate and final receiver (suitable for vacuum operation) allows the separation of the solvent from the product by one-way distillation after reaction. High-quality system components:
Reaction vessels (6, 10, 20 or 30 l)
with thermostatic jacket (heatable by a thermostatic bath), with bottom discharge valve (PTFE), made of DURAN® tubing
Flat flange lid (DN 150 or DN 200)
1 center neck NS 45/40, 2 side necks 45° NS 29/32, 1 side neck straight NS 14/23, material: DURAN®
Feeding funnel
Capacity: 1000 or 4000 ml, with graduation, NS 29/32, made of DURAN® tubing
Spiral condenser
NS 29/32, S 29, jacket length: 300 mm, made of DURAN® tubing
Stirrer guide and stirrer
with 16 mm shaft, stirrer: steel, PTFE coated
| Vessel capacity (l) | Nom. size (DN) | Pack (qty.) | Cat. No. |
|---|---|---|---|
| 6 | 150 | 1 | 6 2654 85 |
| 10 | 150 | 1 | 6 2654 88 |
| 20 | 150 | 1 | 6 2654 94 |
| 6 | 200 | 1 | 6 2655 85 |
| 10 | 200 | 1 | 6 2655 88 |
| 20 | 200 | 1 | 6 2655 94 |
| 30 | 200 | 1 | 6 2655 97 |
Accessories
| Description | Cat. No. |
|---|---|
| Flexible coupling as connection between stirrer and motor | 6 4005 01 |
| Support, for DN 150, complete with connector, approx. W 1,0 x D 0,5 x H 2,0 m |
6 2478 01 |
| Support, for DN 200, complete with connector, approx. W 1,0 x D 0,5 x H 2,0 m |
6 2478 02 |
| Motor, 230 V, with stepless adjustable speed and torque control, digital display |
6 9000 01 |
System contents and spare parts for one-way
reaction/distillation units 6, 10, 20 l, DN 150
Cat. No.: 6 2654 85, Cat.No.: 6 2654 88 and Cat. No.: 6 2654 94
| Pos. | System contents (pc.) | Description | Cat. No. |
|---|---|---|---|
| 1a | 1 | Reaction vessel 6 l, DN 150 | 6 0314 85 |
| 1b | 1 | Reaction vessel 10 l, DN 150 | 6 0314 88 |
| 1c | 1 | Reaction vessel 20 l, DN 150 | 6 0314 94 |
| 2 | 1 | Flat flange lid, DN 150, 1 center neck, 3 side necks | 6 1044 65 |
| 3 | 1 | Stirrer guide, cone NS 45 | 6 3062 06 |
| 4a | 1 | Double-propeller stirrer for 6 l | 6 3310 06 |
| 4b | 1 | Double-propeller stirrer for 10 l | 6 3310 10 |
| 4c | 1 | Double-propeller stirrer for 20 l | 6 3310 20 |
| 5 | 1 | Hinged coupling, metal | 6 4005 01 |
| 6 | 1 | Motor, 230 V | 6 9000 01 |
| 7a | 1 | Dosing funnel 1000 ml, NS 29/32 (for 6 and 10 l) | 6 3500 70 |
| 7b | 1 | Dosing funnel 4000 ml, NS 29/32 (for 20 l) | 6 3500 79 |
| 8 | 1 | Vent tube | 6 3505 04 |
| 9 | 1 | Bend 135°, 2 NS 29/32 | 6 3550 04 |
| 10 | 1 | Distilling head 120° | 6 3551 14 |
| 11 | 1 | Temperature probe Pt 100, 85 mm, NS14/23 | 6 5000 05 |
| 12a | 2 | Flange support, stainless steel, KF 15 (for 6 and 10 l) | 6 2485 15 |
| 12b | 2 | Flange support, stainless steel, KF 25 (for 20 l) | 6 2485 25 |
| 13a | 2 | PTFE-seals KF 15 (for 6 and 10 l) | 6 2488 15 |
| 13b | 2 | PTFE-seals KF 25 (for 20 l) | 6 2488 25 |
| 14a | 2 | Tube adapter KF 15, thread M 16 x 1 (for 6 and 10 l) | 5 1081 10 |
| 14b | 2 | Tube adapter KF 25, thread M 16 x 1 (for 20 l) | 5 1082 16 |
| 15 | 1 | Coil condenser | 5 2550 29 |
| 16 | 1 | Bend, NS 29/32, S 29 | 6 3550 10 |
| 17 | 1 | Intermediate receiver 0.5 l | 6 5150 05 |
| 18 | 1 | Final receiver 2.0 l | 6 5150 10 |
| 19 | 2 | Ventilation valve 0-2.5 mm, NS 29/32 | 6 5200 00 |
| 20 | 1 | Connection valve 10 mm | 6 5200 05 |
| 21 | 10 | Forked clamps NS 29/32 | 1 1035 29 |
| 22 | 1 | Forked clamp S 29 | 1 2329 15 |
| 23 | 1 | Support DN 150, complete with connector | 6 2478 01 |
| 24 | 1 | O-ring, silicone, DN 150 | 6 2480 15 |
| 25a | 1 | Valve plug, 10 mm, PTFE, for 6 l | 6 0613 10 |
| 25b | 1 | Valve plug, 20 mm, PTFE, for 10 and 20 l | 6 0612 20 |
System contents and spare parts for one-way
reaction/distillation units 6, 10, 20, 30 l, DN 200
Cat. No.: 6 2655 85, Cat. No.: 6 2655 88, Cat. No.: 6 2655 94 and 6 2655 97
| Pos. | System contents (pc.) | Description | Cat. No. |
|---|---|---|---|
| 1a | 1 | Reaction vessel 6 l, DN 200 | 6 0315 85 |
| 1b | 1 | Reaction vessel 10 l, DN 200 | 6 0315 88 |
| 1c | 1 | Reaction vessel 20 l, DN 200 | 6 0315 94 |
| 1c | 1 | Reaction vessel 30 l, DN 200 | 6 0315 97 |
| 2 | 1 | Flat flange lid, DN 200, 1 center neck, 3 side necks | 6 1045 65 |
| 3 | 1 | Stirrer guide, cone NS 45 | 6 3062 06 |
| 4a | 1 | Double-propeller stirrer for 6 l | 6 3310 06 |
| 4b | 1 | Double-propeller stirrer for 10 l | 6 3310 10 |
| 4c | 1 | Double-propeller stirrer for 20 l | 6 3310 20 |
| 4c | 1 | Double-propeller stirrer for 30 l | 6 3310 30 |
| 5 | 1 | Hinged coupling, metal | 6 4005 01 |
| 6 | 1 | Motor, 230 V | 6 9000 01 |
| 7a | 1 | Dosing funnel 1000 ml, NS 29/32 (for 6 and 10 l) | 6 3500 70 |
| 7b | 1 | Dosing funnel 4000 ml, NS 29/32 (for 20 and 30 l) | 6 3500 79 |
| 8 | 1 | Vent tube | 6 3505 04 |
| 9 | 1 | Bend 135°, 2 NS 29/32 | 6 3550 04 |
| 10 | 1 | Distilling head 120° | 6 3551 14 |
| 11 | 1 | Temperature probe Pt 100, 85 mm, NS14/23 | 6 5000 05 |
| 12a | 2 | Flange support, stainless steel, KF 15 (for 6 and 10 l) | 6 2485 15 |
| 12b | 2 | Flange support, stainless steel, KF 25 (for 20 and 30 l) | 6 2485 25 |
| 13a | 2 | PTFE-seals KF 15 (for 6 and 10 l) | 6 2488 15 |
| 13b | 2 | PTFE-seals KF 25 (for 20 and 30 l) | 6 2488 25 |
| 14a | 2 | Tube adapter KF 15, thread M 16 x 1 (for 6 and 10 l) | 5 1081 10 |
| 14b | 2 | Tube adapter KF 25, thread M 16 x 1 (for 20 l) | 5 1082 16 |
| 14c | 2 | Tube adapter KF 25, thread M 30 x 1.5 (for 30 l) | 5 1082 30 |
| 15 | 1 | Coil condenser | 5 2550 29 |
| 16 | 1 | Bend, NS 29/32 S 29 | 6 3550 10 |
| 17 | 1 | Intermediate receiver 0.5 l | 6 5150 05 |
| 18 | 1 | Final receiver 2.0 l | 6 5150 10 |
| 19 | 2 | Ventilation valve 0-2.5 mm, NS 29/32 | 6 5200 00 |
| 20 | 1 | Connection valve | 6 5200 05 |
| 21 | 10 | Forked clamps NS 29/32 | 1 1035 29 |
| 22 | 1 | Forked clamp S 29 | 1 2329 15 |
| 23 | 1 | Support DN 200, complete with connector | 6 2478 02 |
| 24 | 1 | O-ring, silicone, DN 200 | 6 2480 20 |
| 25a | 1 | Valve plug, 10 mm, PTFE, for 6 l | 6 0612 10 |
| 25b | 1 | Valve plug, 20 mm, PTFE, for 10, 20 and 30 l | 6 0612 20 |
